3-甲基-3-丁烯-1-醇合成路线 （共 220 条）
反应条件
sulfuric acid T=25°C; effective energy of activation; Rate constantThermodynamic data;
参考文献
Carr, Graham; Whittaker, David
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1989 , p. 359 - 366
反应条件
T=50°C; Zeitlicher Verlauf der Hydratisierung;
参考文献
Eggerer,H.; Lynen,F.
Justus Liebigs Annalen der Chemie, 1960 , vol. 630, p. 58 - 70
反应条件
4-(N,N-dimethlyamino)pyridine; dicyclohexyl-carbodiimide in tetrahydrofuran T=4 - 20°C; 24 h;
参考文献
Bhullar, Khushwant S.; Lassalle-Claux, Gregoire; Touaibia, Mohamed; Vasantha Rupasinghe
European Journal of Pharmacology, 2014 , vol. 730, # 1 p. 125 - 132
反应条件
1: 94 percent / pyridine / 18 h / Ambient temperature 2: 68 percent / Zn(Cu) couple / diethyl ether / 6 h / Heating 3: 63 percent / Zn, AcOH / pyridine / 40 deg C, 2 h, then 70 deg C, 2 h 4: 85 percent / Ba(OH)2 / methanol / 0.5 h / 0 °C View Scheme
参考文献
Aljancic-Solaja, Ivana; Rey, Max; Dreiding, Andre S.
Helvetica Chimica Acta, 1987 , vol. 70, p. 1302 - 1306
反应条件
1: 94 percent / pyridine / 18 h / Ambient temperature 2: 68 percent / Zn(Cu) couple / diethyl ether / 6 h / Heating 3: 63 percent / Zn, AcOH / pyridine / 40 deg C, 2 h, then 70 deg C, 2 h View Scheme
参考文献
Aljancic-Solaja, Ivana; Rey, Max; Dreiding, Andre S.
Helvetica Chimica Acta, 1987 , vol. 70, p. 1302 - 1306
反应条件
palladium diacetate; triethylamine; tris-(o-tolyl)phosphine in acetonitrile Heck Reaction;
参考文献
Byung, Hyun Kim; Jong, Gil Lee; Woon, Ki Kim; Young, Gyu Kim
Organic Process Research and Development, 2005 , vol. 9, # 6 p. 814 - 817
反应条件
1: 200 °C
2: potassium hydrogen sulfate
View Scheme
参考文献
Du Pont de Nemours and Co.
Patent: US2789996 , 1953 ;
反应条件
1: pyridine
2: 15 percent
3: NaH
4: dimethyl copper lithium
View Scheme
参考文献
Lombardo, Domenic A.; Weedon, Alan C.
Tetrahedron Letters, 1986 , vol. 27, # 46 p. 5555 - 5558
参考文献
BASF Aktiengesellschaft
Patent: US4165342 A1, 1979 ;
反应条件
oxygen; ethylenediamine-complexed silver oxalate solution on steatite calcined in air
Product distribution / selectivity;
参考文献
BASF SE
Patent: US2011/15446 A1, 2011 ;
Location in patent: Page/Page column 3-4 ;
