3-甲基-3-丁烯-1-醇合成路线 （共 220 条）
反应条件
indium(III) chloride in dichloromethane
T=20°C; 0.833333 h;
参考文献
Bondalapati, Somasekhar; Reddy, Udagandla C.; Saha, Pipas; Saikia, Anil K.
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 9 p. 3428 - 3438
反应条件
silica gel
T=20°C; 20 h; Yields of byproduct given;
参考文献
Ibatullin, U. G.; Pavlov, Yu. V.; Safarov, M. G.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1989 , vol. 25, # 10 p. 1107 - 1109
Khimiya Geterotsiklicheskikh Soedinenii, 1989 , # 10 p. 1326 - 1328
反应条件
toluene-4-sulfonic acid in benzene
T=20 - 25°C; 20 h; Product distributionMechanism;
参考文献
Gevorkyan, A.A.; Arakelyan, A.S.; Kazaryan, P.I.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1982 , vol. 18, # 12 p. 1240 - 1242
Khimiya Geterotsiklicheskikh Soedinenii, 1982 , vol. 18, # 12 p. 1611 - 1613
反应条件
boron trifluoride diethyl etherate in benzene
T=20°C; 0.5 h;
参考文献
Bondalapati, Somasekhar; Reddy, Udagandla C.; Saha, Pipas; Saikia, Anil K.
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 9 p. 3428 - 3438
反应条件
indium(III) chloride in dichloromethane
T=20°C; 0.833333 h;
参考文献
Bondalapati, Somasekhar; Reddy, Udagandla C.; Saha, Pipas; Saikia, Anil K.
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 9 p. 3428 - 3438
反应条件
silica gel
T=20°C; 20 h; Yields of byproduct given;
参考文献
Ibatullin, U. G.; Pavlov, Yu. V.; Safarov, M. G.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1989 , vol. 25, # 10 p. 1107 - 1109
Khimiya Geterotsiklicheskikh Soedinenii, 1989 , # 10 p. 1326 - 1328
反应条件
sodium hydrogen sulphate in water; toluene
T=110 - 115°C; 21.5 h;
参考文献
BASF SE
Patent: US2010/311988 A1, 2010 ;
Location in patent: Page/Page column 4 ;
反应条件
sodium hydrogen sulphate in water; toluene
T=110 - 115°C; 21.5 h; Dean-Stark;
参考文献
BASF SE; Heidemann, Thomas; Königsmann, Lucia
Patent: US2013/109867 A1, 2013 ;
Location in patent: Paragraph 0083 ;
反应条件
triethylamine
1.) 30 min, 70 deg C, 2.) 12 h, room temperature;
参考文献
Julia, M.; Schmitz, C.
Bulletin de la Societe Chimique de France, 1986 , # 4 p. 630 - 636
反应条件
1: 71 percent / pNO2-perbenzoicacid / CHCl3 / 2 h / Ambient temperature
2: 1.)Bu3SnOMe 3.)m-Ph(COOH)2
View Scheme
参考文献
Bats, J. -P.; Moulines, J.; Picard, P.; Leclercq, D.
Tetrahedron, 1982 , vol. 38, # 14 p. 2139 - 2146
