3-甲基-3-丁烯-1-醇合成路线 （共 220 条）
反应条件
2,2'-azo-bisisobutyronitrile
参考文献
Sharma,N.K. et al.
Canadian Journal of Chemistry, 1976 , vol. 54, p. 3012 - 3025
反应条件
1: AIBN
2: tBuOCl / methanol
View Scheme
参考文献
Sharma,N.K. et al.
Canadian Journal of Chemistry, 1976 , vol. 54, p. 3012 - 3025
反应条件
2: 92 percent / Amberlyst A 26 (OH- form) / methanol / 2 h / Ambient temperature
3: 84 percent / Amberlyst A 26 (CO32- form) / benzene / 6 h / Heating
View Scheme
参考文献
Bongini, Alessandro; Cardillo, Giuliana; Orena, Mario; Porzi, Gianni; Sandri, Sergio
Journal of Organic Chemistry, 1982 , vol. 47, # 24 p. 4626 - 4633
反应条件
aluminum oxide
T=20°C; 20 h; Yields of byproduct given;
参考文献
Ibatullin, U. G.; Pavlov, Yu. V.; Safarov, M. G.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1989 , vol. 25, # 10 p. 1107 - 1109
Khimiya Geterotsiklicheskikh Soedinenii, 1989 , # 10 p. 1326 - 1328
反应条件
NaA (4 Angstroem)
T=20°C; 20 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Ibatullin, U. G.; Pavlov, Yu. V.; Safarov, M. G.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1990 , vol. 26, # 2 p. 155 - 157
Khimiya Geterotsiklicheskikh Soedinenii, 1990 , vol. 26, # 2 p. 183 - 186
反应条件
1: Et3N
2: TMSOTf, collidine / CCl4 / 25 °C
View Scheme
参考文献
Mekhalfia; Marko; Adams
Tetrahedron Letters, 1991 , vol. 32, # 36 p. 4783 - 4786
反应条件
aluminum oxide
T=20°C; 20 h;
参考文献
Ibatullin, U. G.; Pavlov, Yu. V.; Safarov, M. G.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1989 , vol. 25, # 10 p. 1107 - 1109
Khimiya Geterotsiklicheskikh Soedinenii, 1989 , # 10 p. 1326 - 1328
反应条件
sulfuric acid
T=25°C;
参考文献
Margot, Christian; Schlosser, Manfred
Tetrahedron Letters, 1985 , vol. 26, # 8 p. 1035 - 1038
反应条件
methanesulfonic acid
T=60°C; 6 h;
参考文献
KAO CORPORATION
Patent: EP1493737 A1, 2005 ;
Location in patent: Page/Page column 6 ;
反应条件
aluminum oxide
T=20°C; 20 h;
参考文献
Ibatullin, U. G.; Pavlov, Yu. V.; Safarov, M. G.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1989 , vol. 25, # 10 p. 1107 - 1109
Khimiya Geterotsiklicheskikh Soedinenii, 1989 , # 10 p. 1326 - 1328
