in water neutralization of an aq. soln. of MoO3 with Na2CO3;; evapn. at ambient temp.;;

in sodium hydroxide byproducts: NH3; addn. of an excess of NaOH to a soln. of ammonium molybdate; boiling til formation of NH3 stops;; addn. of alc.; pptn.; washing with alc.; drying; recrystn. from H2O;;

in water solving of Na2MoO4 in H2O;; concn. of the soln.; crystn.; filtration; washing with small amt. of H2O; drying between paper and then over CaO and H2SO4 for 24 hours;;

hydrogenchloride in water according to: F. W. Moore and M. L. Larson, Inorg. Chem. 1967, 6, 998., adding HCl; filtn., washing (H2O), drying, recrystallization (Et2O, benzene);

sodium hydroxide; sodium chloride; dihydrogen peroxide in water; acetonitrile

NaCH3COO; hydrochloric acid in water to aq. soln. of Na2MoO4*2H2O, (NEt2H2)(S2CPh), and MeCO2Na added HCl (1.0 M) dropwise with stirring at room temp.; ppt. filtered off, washed with water and methanol, dried in vac., chromd. (SiO2, CS2), orange fraction evapd. in vac., recrystd. from CH2Cl2-light petroleum; elem. anal.;

1: in ethylene glycol 2 h; 2: With ethylenediamine in ethylene glycol T=160°C; 6.5 h; Autoclave; TemperatureReagent/catalyst;

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sodium hydroxide in CS2