in neat (no solvent) byproducts: NaF; mixt. of NaNO3 (excess) and ClF in a stainless steel cylinder allowed to warm slowly in a dry-ice-liquid N2 slush bath from -196°VC to -78 and then toward 0°C, recooled to -196°C; fractional condensation;
参考文献
Christe, Karl O.; Wilson, William W.; Wilson, Richard D.
Inorganic Chemistry, 1989 , vol. 28, p. 675 - 677
in neat (no solvent) byproducts: Cl2, NaF; finely powdered NaNO3 loaded into a stainless steeel cylinder, ClF (excess) added at -196°C, cylinder allowed to warm slowly to room temp., kept for 3d, cooled to -196°C; fractional condensation;
参考文献
Christe, Karl O.; Wilson, William W.; Wilson, Richard D.
Inorganic Chemistry, 1989 , vol. 28, p. 675 - 677
in neat (no solvent) addn. of concd. H2SO4 to solid NaNO3; vac. distn. (77 K);
参考文献
Volney, C. W.
Journal of the American Chemical Society, 1901 , vol. 23, p. 489
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Uebel
Patent: DE277092 , 1913 ;
