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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
76311-47-2
合成路线
（共 18 条）
108-05-4
醋酸乙烯酯
+
76311-47-2
→
反应条件
1092080-61-9
+
1335545-22-6
+
1335545-21-5
+
529-34-0
1-四氢萘酮
反应条件
immobilized Candida antarctica lipase A in toluene 144 h; optical yield given as percent eeenantioselective reaction;
参考文献
Rodriguez-Rodriguez, Jesus A.; Gotor, Vicente; Brieva, Rosario
Tetrahedron Asymmetry, 2011 , vol. 22, # 11 p. 1218 - 1224
76311-47-2
→
反应条件
1335545-25-9
+
529-34-0
1-四氢萘酮
反应条件
1: pyridine / dichloromethane / 4 h / 20 °C / Inert atmosphere 2: immobilized Candida antarctica lipase A; water / 1,4-dioxane / 5 h / 40 °C / pH 5 / Citrate buffer; Enzymatic reaction View Scheme
参考文献
Rodriguez-Rodriguez, Jesus A.; Gotor, Vicente; Brieva, Rosario
Tetrahedron Asymmetry, 2011 , vol. 22, # 11 p. 1218 - 1224
76311-47-2
→
反应条件
1335545-31-7
+
529-34-0
1-四氢萘酮
反应条件
1: pyridine / dichloromethane / 12 h / 20 °C / Inert atmosphere 2: immobilized Candida antarctica lipase A; 1,2,3,4-tetrahydro-1-naphthylamine / diethyl ether / 23 h / 30 °C / Enzymatic reaction View Scheme
参考文献
Rodriguez-Rodriguez, Jesus A.; Gotor, Vicente; Brieva, Rosario
Tetrahedron Asymmetry, 2011 , vol. 22, # 11 p. 1218 - 1224
76311-47-2
→
反应条件
1092080-61-9
+
1335545-22-6
+
529-34-0
1-四氢萘酮
反应条件
1: pyridine / dichloromethane / 4 h / 20 °C / Inert atmosphere 2: immobilized Pseudomonas cepacia lipase; water / 1,4-dioxane / 156 h / 30 °C / Enzymatic reaction View Scheme
参考文献
Rodriguez-Rodriguez, Jesus A.; Gotor, Vicente; Brieva, Rosario
Tetrahedron Asymmetry, 2011 , vol. 22, # 11 p. 1218 - 1224
76311-47-2
→
反应条件
1335545-25-9
反应条件
1: pyridine / dichloromethane / 4 h / 20 °C / Inert atmosphere 2: immobilized Pseudomonas cepacia lipase; water / 1,4-dioxane / 30 °C / pH 5 / Citrate buffer; Enzymatic reaction View Scheme
参考文献
Rodriguez-Rodriguez, Jesus A.; Gotor, Vicente; Brieva, Rosario
Tetrahedron Asymmetry, 2011 , vol. 22, # 11 p. 1218 - 1224
76311-47-2
→
反应条件
1335545-31-7
反应条件
1: pyridine / dichloromethane / 12 h / 20 °C / Inert atmosphere 2: immobilized Pseudomonas cepacia lipase; water / 1,4-dioxane / 312 h / 30 °C / pH 5 / Citrate buffer; Enzymatic reaction View Scheme
参考文献
Rodriguez-Rodriguez, Jesus A.; Gotor, Vicente; Brieva, Rosario
Tetrahedron Asymmetry, 2011 , vol. 22, # 11 p. 1218 - 1224
76311-47-2
→
反应条件
1335545-31-7
+
529-34-0
1-四氢萘酮
反应条件
1.1: pyridine / dichloromethane / 12 h / 20 °C / Inert atmosphere 2.1: immobilized Pseudomonas cepacia lipase; water / diethyl ether / 16 h / 30 °C / Enzymatic reaction 2.2: 6 h / 20 °C View Scheme
参考文献
Rodriguez-Rodriguez, Jesus A.; Gotor, Vicente; Brieva, Rosario
Tetrahedron Asymmetry, 2011 , vol. 22, # 11 p. 1218 - 1224
76311-47-2
→
反应条件
529-34-0
1-四氢萘酮
反应条件
1.1: pyridine / dichloromethane / 4 h / 20 °C / Inert atmosphere 2.1: immobilized Pseudomonas cepacia lipase; water / 1,4-dioxane / 156 h / 30 °C / Enzymatic reaction 2.2: 6 h / 20 °C View Scheme
参考文献
Rodriguez-Rodriguez, Jesus A.; Gotor, Vicente; Brieva, Rosario
Tetrahedron Asymmetry, 2011 , vol. 22, # 11 p. 1218 - 1224
76311-47-2
→
反应条件
1092080-61-9
+
1335545-22-6
+
1335545-31-7
+
529-34-0
1-四氢萘酮
反应条件
1: pyridine / dichloromethane / 12 h / 20 °C / Inert atmosphere 2: immobilized Candida antarctica lipase A; water / diethyl ether / 2 h / 30 °C / Enzymatic reaction View Scheme
参考文献
Rodriguez-Rodriguez, Jesus A.; Gotor, Vicente; Brieva, Rosario
Tetrahedron Asymmetry, 2011 , vol. 22, # 11 p. 1218 - 1224
76311-47-2
→
反应条件
1335545-22-6
+
1335545-31-7
反应条件
1: pyridine / dichloromethane / 12 h / 20 °C / Inert atmosphere 2: immobilized Pseudomonas cepacia lipase; water / diethyl ether / 16 h / 30 °C / Enzymatic reaction View Scheme
参考文献
Rodriguez-Rodriguez, Jesus A.; Gotor, Vicente; Brieva, Rosario
Tetrahedron Asymmetry, 2011 , vol. 22, # 11 p. 1218 - 1224
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