暂无反应条件数据

1: 76 percent / p-toluenesulphonic acid / benzene / Heating 2: 75 percent / 1) LAH / diethyl ether / Ambient temperature 3: 75 percent / LAH / diethyl ether 4: 50 percent / mercuric acetate / 10 h / Heating 5: 0.5 h / 185 - 190 °C 6: 70 percent / 1.) r. t. overnight 2.) 3 h 50 deg C 7: 74 percent / PTS / benzene / 6 h / Heating 8: H2O / PTS / acetone / 24 h / Ambient temperature 9: 79 percent / diethyl ether / 1.) 8 h 2.) reflux 2 h View Scheme

1: 76 percent / p-toluenesulphonic acid / benzene / Heating 2: 75 percent / 1) LAH / diethyl ether / Ambient temperature 3: 75 percent / LAH / diethyl ether 4: 50 percent / mercuric acetate / 10 h / Heating View Scheme

1: 90 percent / potassium carbonate / acetone / 6 h / Heating 2: 1.) n-butyllithium / 1.) THF, hexane, -65 - 0 deg C, 2.) -65 deg C up to room temp., 1 h 3: 1 N H2SO4 / acetone / 0.5 h 4: LiAlH4 / diethyl ether / 3 h / Ambient temperature 5: pyridine / diethyl ether / 2 h / Ambient temperature 6: 99 percent / CH2Cl2 / 1 h / Ambient temperature 7: sodium methoxide / CH2Cl2; methanol / 0.17 h / 0 - 5 °C 8: triethylamine / bis(benzonitrile)palladium dichloride / acetonitrile / 1 h / Ambient temperature 9: potassium hydroxide / methanol; H2O / 0.5 h / Heating View Scheme