反应条件
in further solvent(s) solvent: anhydrous HF;BF3 and solvent condensed on KAgF4 at -196 ° C, gas admitted slowly to promote crystallinity of product, mixture warmed, at ca. -40 ° C: pptn.; KBF4 removed by washing via decantation of the soln., product contaminated with KBF4;
参考文献
Zemva, Boris; Lutar, Karel; Jesih, Adolf; Casteel Jr., William J.; Wilkinson, Angus P.; Cox, David E.; Von Dreele, Robert B.; Borrmann, Horst; Bartlett, Neil
Journal of the American Chemical Society, 1991 , vol. 113, # 11 p. 4192 - 4198
