Burg; Banus
Journal of the American Chemical Society, 1954 , vol. 76, p. 3903
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Gmelin Handbook: B: B-Verb.4, 4.4.1, page 110 - 117
in neat (no solvent) equimolar amt. of BF3 and (CH3)2NH were distd. into a bulb cooled in liq. N2, the bulb was isolated and allowed to warm slowly , the react. mixt. was cooled at intervals; pumped at room temp. to remove excess reactants and volatile products;
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Kroto, Harold W.; McNaughton, Donald
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1985 , p. 1767 - 1770
in solid matrix onto a frozen soln. of Me3SiNMe2 in SO2 in an NMR-tube BF3 is condensed at -196°C, warming up to room temp.; monitored by NMR-spectroscopy;
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Tornieporth-Oetting, I. C.; Klapoetke, T. M.
Polyhedron, 1992 , vol. 11, p. 2183 - 2186
