反应条件
in neat (no solvent) byproducts: (CH3)4NHBF3; BF3 condensing under N2 at -196°C onto ammonium salt, warming to0°C, stirring for 3 h, cooling to -196°C, warming slowly to room temp. while the volatiles pumping off, borane collecting at -140°C; identified by IR spectrum;
参考文献
Inorganic Chemistry, , vol. 21, p. 1952 - 1957
