N,N′-二戊基-3,4,9,10-苝二甲酰亚胺合成路线 （共 3 条）
反应条件
1.1: sulfuryl dichloride; iodobenzene; iodine / nitrobenzene / 8 h / 80 - 85 °C 2.1: potassium carbonate / 1-methyl-pyrrolidin-2-one / 14 h / 130 °C / Inert atmosphere 3.1: potassium hydroxide / tert-butyl alcohol / Heating 3.2: Acidic aq. solution View Scheme
参考文献
Perrin, Lara; Hudhomme, Pietrick
European Journal of Organic Chemistry, 2011 , # 28 p. 5427 - 5440
反应条件
in N,N-dimethyl-formamide
4 h; Reflux;
参考文献
Perrin, Lara; Hudhomme, Pietrick
European Journal of Organic Chemistry, 2011 , # 28 p. 5427 - 5440
反应条件
in water
T=60°C; 3.5 h;
参考文献
Nagao, Yukinori; Misono, Takahisa
Bulletin of the Chemical Society of Japan, 1981 , vol. 54, # 4 p. 1191 - 1194
