D-赤式-二氢-D-鞘氨醇合成路线 (共 64 条)
反应条件
hydrogen; 10percent Pd/C in methanol T=24°C; Catalytic hydrogenation; P=760.051 Torr; 7.5 h;
参考文献
Nicholas, Gillian M.; Molinski, Tadeusz F.
Journal of the American Chemical Society, 2000 , vol. 122, # 17 p. 4011 - 4019
反应条件
hydrogenchloride; palladium on carbon; hydrogen in ethyl acetate T=320°C; 48 h;
参考文献
Mettu, Ravinder; Thatikonda, Narendar Reddy; Olusegun, Oladoye Sunday; Vishvakarma, Ramesh; Vaidya, Jayathirtha Rao
Arkivoc, 2012 , vol. 2012, # 6 p. 421 - 436
反应条件
hydrogenchloride in ethyl acetate 0.5 h;
参考文献
Mori, Kenji; Uenishi, Keiji
Liebigs Annalen der Chemie, 1994 , # 1 p. 41 - 48
反应条件
hydrogenchloride in 1,4-dioxane; methanol T=20°C; 0.5 h;
参考文献
Zhong, Yu-Wu; Dong, Yi-Zhou; Fang, Kai; Izumi, Kenji; Xu, Ming-Hua; Lin, Guo-Qiang
Journal of the American Chemical Society, 2005 , vol. 127, # 34 p. 11956 - 11957
反应条件
hydrogen; acetic acid in methanol T=20°C; P=3102.97 Torr; 8 h;
参考文献
Pandey, Menaka; Chowdhury, Partha Sarathi; Dutta, Achintya Kumar; Kumar, Pradeep; Pal, Sourav
RSC Advances, 2013 , vol. 3, # 35 p. 15442 - 15448
反应条件
lithium aluminium tetrahydride in tetrahydrofuran T=63 - 65°C; Reduction; 2 h;
参考文献
He, Linli; Byun, Hoe-Sup; Bittman, Robert
Journal of Organic Chemistry, 2000 , vol. 65, # 22 p. 7618 - 7626
反应条件
hydrogen; palladium on activated charcoal in ethanol Reduction; P=760 Torr; 3 h;
参考文献
Kobayashi, Shu; Furuta, Takayuki
Tetrahedron, 1998 , vol. 54, # 35 p. 10275 - 10294
反应条件
dimethylsulfide borane complex in tetrahydrofuran T=-78 - 20°C; 2.16667 h; Inert atmosphere; enantioselective reaction;
参考文献
Devi, Thongam Joymati; Saikia, Bishwajit; Barua, Nabin C.
Tetrahedron, 2013 , vol. 69, # 19 p. 3817 - 3822
反应条件
hydrogen; trifluoroacetic acid; palladium on activated charcoal in methanol T=20°C; P=3800.26 Torr; 28 h;
参考文献
Tetrahedron Letters, , vol. 49, # 32 p. 4728 - 4730
反应条件
trifluoroacetic acid in water 1 h;
参考文献
Mun, JiYoung; Onorato, Amber; Nichols, Frank C.; Morton, Martha D.; Saleh, Abdullah I.; Welzel, Morgan; Smith, Michael B.
Organic and Biomolecular Chemistry, 2007 , vol. 5, # 23 p. 3826 - 3833