D-赤式-二氢-D-鞘氨醇合成路线 （共 64 条）
反应条件
borane-ammonia complex; lithium diisopropyl amide in tetrahydrofuran; hexane T=0 - 25°C; Inert atmosphere;
参考文献
Sarabia, Francisco; Vivar-Garcia, Carlos; Garcia-Castro, Miguel; Garcia-Ruiz, Cristina; Martin-Galvez, Francisca; Sanchez-Ruiz, Antonio; Chammaa, Samy
Chemistry - A European Journal, 2012 , vol. 18, # 47 p. 15190 - 15201
反应条件
lithium aluminium tetrahydride in tetrahydrofuran 72 h; Heating;
参考文献
Cai, Ye; Ling, Chang-Chun; Bundle, David R.
Organic and Biomolecular Chemistry, 2006 , vol. 4, # 6 p. 1140 - 1146
反应条件
2: 1N HCl, cyclohexene / 10percent Pd/C / methanol / 2 h / Heating View Scheme
参考文献
Journal of Organic Chemistry, , vol. 50, # 20 p. 3752 - 3757
反应条件
lithium hydroxide; ammonia; sodium; sodium hydride Multistep reaction;
参考文献
Journal of Organic Chemistry, , vol. 50, # 20 p. 3752 - 3757
反应条件
hydrogen sulfide in pyridine; water 4 h; Ambient temperature;
参考文献
Wild, Robert; Schmidt, Richard R.
Liebigs Annalen, 1995 , # 5 p. 755 - 764
反应条件
1: 94 percent / naphthalene; Li / tetrahydrofuran / 0 - 20 °C 2: 98 percent / HCl / methanol; dioxane / 0.5 h / 20 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 127, # 34 p. 11956 - 11957
反应条件
1: 64 percent Turnov. / SmI2; t-BuOH / tetrahydrofuran / 13 h / -78 °C 2: 94 percent / naphthalene; Li / tetrahydrofuran / 0 - 20 °C 3: 98 percent / HCl / methanol; dioxane / 0.5 h / 20 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 127, # 34 p. 11956 - 11957
反应条件
hydrogen; palladium on activated charcoal in acetic acid
参考文献
Journal of Organic Chemistry, , vol. 35, # 10 p. 3521 - 3524
反应条件
hydrogenchloride; cyclohexene; palladium on activated charcoal in methanol 2 h; Heating;
参考文献
Journal of Organic Chemistry, , vol. 50, # 20 p. 3752 - 3757
反应条件
hydrogenchloride in tetrahydrofuran
参考文献
Cook, Gregory R.; Pararajasingham, Ketheeswaran
Tetrahedron Letters, 2002 , vol. 43, # 50 p. 9027 - 9029
