1: 3-methoxy-4-hydroxybenzylamine hydrochloride With sodium hydroxide in water; N,N-dimethyl-formamide T=20°C; 1 h; Inert atmosphereCooling with ice; 2: n-nonanoic acid chloride in tetrahydrofuran; water; N,N-dimethyl-formamide T=20°C; 18 h; Inert atmosphereCooling with ice;
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Barbero, Gerardo F.; Molinillo, Jose M. G.; Varela, Rosa M.; Palma, Miguel; MacIas, Francisco A.; Barroso, Carmelo G.
Journal of Agricultural and Food Chemistry, 2010 , vol. 58, # 6 p. 3342 - 3349
aluminium trichloride in dichloromethane 4 h; Heating;
参考文献
Neubert, Mary E.; Herlinger, Frank C.; Jirousek, Michael R.; Vries, Adriaan De
Molecular Crystals and Liquid Crystals (1969-1991), 1986 , vol. 139, p. 299 - 320
1: 89.8 percent / Et3N / CH2Cl2 / 1.5 h / Heating 2: 60.5 percent / H2 / 10percent Pd-C / ethanol / 1 h / Ambient temperature View Scheme
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Neubert, M. E.; Keast, S. S.; Ezenyilimba, M. C.; Greer, P. B.; Jones, W. C.; et al.
Molecular Crystals and Liquid Crystals Science and Technology, Section A: Molecular Crystals and Liquid Crystals, 1993 , vol. 237, p. 47 - 68
