2-(4-甲氧基苯基)-1-丙-2-基-6,7-二氢-5H-吲哚-4-酮合成路线 （共 7 条）
反应条件
in methanol
T=20°C; Morita-Baylis-Hillman reaction; 0.5 h;
参考文献
Batchu, Harikrishna; Batra, Sanjay
European Journal of Organic Chemistry, 2012 , # 15 p. 2935 - 2944
反应条件
1.1: pyridine / dichloromethane / 0 °C
1.2: 0 - 20 °C
2.1: methanol / 0.5 h / 20 °C
View Scheme
参考文献
Batchu, Harikrishna; Batra, Sanjay
European Journal of Organic Chemistry, 2012 , # 15 p. 2935 - 2944
反应条件
1.1: 4-(N,N-dimethlyamino)pyridine / tetrahydrofuran; water / 20 °C
2.1: pyridine / dichloromethane / 0 °C
2.2: 0 - 20 °C
3.1: methanol / 0.5 h / 20 °C
View Scheme
参考文献
Batchu, Harikrishna; Batra, Sanjay
European Journal of Organic Chemistry, 2012 , # 15 p. 2935 - 2944
反应条件
1.1: selenium(IV) oxide / 1,4-dioxane; water / 70 °C
2.1: 4-(N,N-dimethlyamino)pyridine / tetrahydrofuran; water / 20 °C
3.1: pyridine / dichloromethane / 0 °C
3.2: 0 - 20 °C
4.1: methanol / 0.5 h / 20 °C
View Scheme
参考文献
Batchu, Harikrishna; Batra, Sanjay
European Journal of Organic Chemistry, 2012 , # 15 p. 2935 - 2944
反应条件
in acetic acid
0.666667 h; Heating;
参考文献
Shvedov, V. I.; Safonova, O. A.; Bulanova, T. I.; Il'ina, A. S.; Shvarts, G. Ya.; et al.
Pharmaceutical Chemistry Journal, 1980 , vol. 14, # 11 p. 794 - 798
Khimiko-Farmatsevticheskii Zhurnal, 1980 , vol. 14, # 11 p. 67 - 71
反应条件
1: 53 percent / aq. KOH / various solvent(s) / Ambient temperature
2: 52 percent / acetic acid / 0.67 h / Heating
View Scheme
参考文献
Shvedov, V. I.; Safonova, O. A.; Bulanova, T. I.; Il'ina, A. S.; Shvarts, G. Ya.; et al.
Pharmaceutical Chemistry Journal, 1980 , vol. 14, # 11 p. 794 - 798
Khimiko-Farmatsevticheskii Zhurnal, 1980 , vol. 14, # 11 p. 67 - 71
反应条件
1: 53 percent / aq. KOH / various solvent(s) / Ambient temperature
2: 52 percent / acetic acid / 0.67 h / Heating
View Scheme
参考文献
Shvedov, V. I.; Safonova, O. A.; Bulanova, T. I.; Il'ina, A. S.; Shvarts, G. Ya.; et al.
Pharmaceutical Chemistry Journal, 1980 , vol. 14, # 11 p. 794 - 798
Khimiko-Farmatsevticheskii Zhurnal, 1980 , vol. 14, # 11 p. 67 - 71
