1: diazomethyl-trimethyl-silane With n-butyllithium in tetrahydrofuran; hexane
T=-78°C; 1 h;
2: benzaldehyde; methyl iodide in tetrahydrofuran; hexane
T=-78°C; 2.3 h;
3: With dirhodium tetraacetate in tetrahydrofuran; hexane
T=-78 - 20°C; 0.25 h; Further stages.;
参考文献
Aggarwal, Varinder K.; Sheldon, Chris G.; Macdonald, Gregor J.; Martin, William P.
Journal of the American Chemical Society, 2002 , vol. 124, # 35 p. 10300 - 10301
