in diethyl ether; benzene addn. of 1.5 molar iso-C3H7MgCl soln. to an icy cold SnCl4 soln. during 3 h, molar ratio of iso-C3H7MgCl:SnCl4=4:1, standing for overnight, then addn. of water; purifn. with NaOH, then distn.;
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Ladenburg, A.
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Gmelin Handbook: Sn: Org.Verb.2, 1.1.2.2.9, page 238 - 244