in neat (no solvent) Ar atmosphere; reaction of org. compd. and SnCl4 (10 h, 45°C); not sepd.;
参考文献
Muratova, A. A.; Sobanova, O. B.; Yarkova, E. G.; Sarycheva, T. I.; Khramov, A. S.; Pudovik, A. N.
Journal of General Chemistry USSR (English Translation), 1980 , vol. 50, p. 410 - 417
Zhurnal Obshchei Khimii, 1980 , vol. 50, p. 518 - 527
in pentane Ar atmosphere; reaction of org. compd. and SnCl4 in pentane (2 month, 0°C); filtration, washing, drying (vac.); melting point;
参考文献
Muratova, A. A.; Sobanova, O. B.; Yarkova, E. G.; Sarycheva, T. I.; Khramov, A. S.; Pudovik, A. N.
Journal of General Chemistry USSR (English Translation), 1980 , vol. 50, p. 410 - 417
Zhurnal Obshchei Khimii, 1980 , vol. 50, p. 518 - 527
in neat (no solvent) Ar atmosphere; reaction of org. compd. and SnCl4 (10 h, 45°C); not sepd.;
参考文献
Muratova, A. A.; Sobanova, O. B.; Yarkova, E. G.; Sarycheva, T. I.; Khramov, A. S.; Pudovik, A. N.
Journal of General Chemistry USSR (English Translation), 1980 , vol. 50, p. 410 - 417
Zhurnal Obshchei Khimii, 1980 , vol. 50, p. 518 - 527
sodium in Petroleum ether (Ar); vigorous stirred suspn. of Na was maintained at 115°C for 0.5 h, one drop of SnCl4 was added and ClC4H9 was added dropwise within 3 h at 30-40°C, after 1 h stirring SnCl4 (4:1 mol) was dropped into mixt. (same temp.) within 75 min; after stirring for a further h at 30-40°C mixt. was filtered off and residue treated with tBuOH, solvents were distd. off from filtrate; identification by GC after methylation;
参考文献
Journal of Organometallic Chemistry, , vol. 255, # 2 p. 173 - 178
in pentane Ar atmosphere; reaction of org. compd. and SnCl4 in pentane, keeping for 2 month at 0°C; filtration, dissolution (CH2Cl2), filtration, drying (vac.); melting point, IR spectroscopy;
参考文献
Muratova, A. A.; Sobanova, O. B.; Yarkova, E. G.; Sarycheva, T. I.; Khramov, A. S.; Pudovik, A. N.
Journal of General Chemistry USSR (English Translation), 1980 , vol. 50, p. 410 - 417
Zhurnal Obshchei Khimii, 1980 , vol. 50, p. 518 - 527
in neat (no solvent) Ar atmosphere; addn. of SnCl4 and ethyl phosphorodichloridite to (EtO)3P with stirring and cooling (-15 - (-10)°C), heating (10 h, 45°C); not sepd.; Moesbauer spectroscopy;
参考文献
Muratova, A. A.; Sobanova, O. B.; Yarkova, E. G.; Sarycheva, T. I.; Khramov, A. S.; Pudovik, A. N.
Journal of General Chemistry USSR (English Translation), 1980 , vol. 50, p. 410 - 417
Zhurnal Obshchei Khimii, 1980 , vol. 50, p. 518 - 527
Dey, A. K.; Bhattacharya, A. K.
Journal of the Indian Chemical Society, 1948 , vol. 25, p. 571 - 574
Full Text Show Details
Gmelin Handbook: Sn: MVol.C2, 14.18, page 224 - 225
in hexane; benzene a mixt. of Cp2ZrHCl and 1-octene in benzene was stirred for ca. 2 h at room temp. under N2, a soln. of anhyd. SnCl4 in n-hexane was added dropwise (Cp2ZrHCl/SnCl4 ratio 2:1), stirred for a further 1 h 30 min; hexane was added, ppt. of Cp2ZrCl2 was filtered off, filtrate was concd., residue extd. with hexane, exts. were combined, concd., dild. with methanol; (octyl)SnCl3 content was detd. by titrn. with 0.02 M EDTA;
参考文献
Das, V. G. Kumar; Chee, Ong Ghee
Journal of Organometallic Chemistry, 1987 , vol. 321, p. 335 - 338
