反应条件
AlCl3 in neat (no solvent) slow heating of a mixt. of Sn-compd., SnCl4 and AlCl3 to 210°C under N2, keeping at this temp. for 4 h; cooling to room temp., addn. of Et2O, filtn., cooling to 0°C, crystn., recrystn. from n-hexane, evapn. of mother liquor yields second crop, elem. anal.;
参考文献
Schenk, Wolfdieter A.; Khadra, Almuetassem; Burschka, Christian
Journal of Organometallic Chemistry, 1994 , vol. 468, # 1-2 p. 75 - 86
