sodium hydroxide in water N2 atmosphere; 25°C, ionic strength 0.2 (NaCl); no isolation; monitoring by potentiometric titration;
参考文献
Vasil'ev, V. P.; Zaitseva, G. A.
Russian Journal of Inorganic Chemistry (Translation of Zhurnal Neorganicheskoi Khimii), 1989 , vol. 34, p. 1761 - 1763
Zhurnal Neorganicheskoi Khimii, 1989 , vol. 34, p. 3082 - 3086
sodium hydroxide in water N2 atmosphere; 25°C, ionic strength 0.2 (NaCl), pH 5-9; no isolation; monitoring by potentiometric titration;
参考文献
Vasil'ev, V. P.; Zaitseva, G. A.
Russian Journal of Inorganic Chemistry (Translation of Zhurnal Neorganicheskoi Khimii), 1989 , vol. 34, p. 1761 - 1763
Zhurnal Neorganicheskoi Khimii, 1989 , vol. 34, p. 3082 - 3086
in not given in an inert atmosphere (free of O2); mixing of metal compd. and amino acid as aq. solns. (H2O, D2O, pH 3.7-11.0); not isolated; detn. by NMR;;
参考文献
Tikhonov, V. P.
Sov. J. Coord. Chem. (Engl. Transl.), 1991 , vol. 17, p. 581 - 587
Koordinatsionnaya Khimiya, 1991 , vol. 17, p. 1094 - 1100
dihydrogen peroxide in water to ice-cooled soln. of CoCl2 in NaHCO3 H2O2 added dropwise, Co(NH3)6Co(CO3)3 added; ppt. sepd., washed (ice-cold water), dried (dessicator);
参考文献
Ermolaev, V. M.; Zakharova, E. V.; Shilov V. P.
Radiochemistry (Moscow), 2001 , vol. 43, p. 424 - 428
Radiokhimiya, 2001 , vol. 43, p. 374 - 377
Bi(Si(CH3)3)3 in tetrahydrofuran upon addn. of Bi(Si(CH3)3)3 to anhydrous CoCl2 in the presence of P(C6H5)3 in tetrahydrofuran soln.;; green crystals of CoCl(P(C6H5)3)3 and blue crystals of CoCl2(P(C6H5)3)2 (determined by comparison of X-ray powder cell parameters) were obtained;
参考文献
Cassidy, Juanita M.; Whitmire, Kenton H.
Acta Crystallographica, Section C: Crystal Structure Communications, 1991 , vol. 47, p. 2094 - 2098