in ethanol soln. of 1,10-phenanthroline monohydrate in EtOH added to soln. of ZnCl2in EtOH; after 0.5 h ppt. filtered off; washed (EtOH); dried at room temp. for 0.5 h; elem. anal.;
参考文献
Skogareva; Minacheva; Sergienko; Minaeva; Filippova
Russian Journal of Inorganic Chemistry, 2004 , vol. 49, # 6 p. 853 - 862
s-BuLi in tetrahydrofuran; diethyl ether; hexane at -110°C, CF2CH2 + s-BuLi in hexane, THF-Et2O (4:1), stirring (20 min), then ZnCl2 added to the mixt., stirring (-100°C, 30 min); (19)F NMR;
