in water High Pressure; mixing urea and solns. of zinc compd. and aluminium compd. with stirring, heating; different temp. and heating time were used; cooling to room temp., centrifugation, washing with distd. water, dryingat 40°C in air, XRD;
in not given a 2:1 mixt. of MnCl2 and ZnCl2 is molten together with KClO4;;
参考文献
Gooch; Kreider
Z. Anorg. Chem., 1895 , vol. 10, p. 277 - 277
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Gooch; Kreider
Z. Anorg. Chem., 1894 , vol. 7, p. 13 - 13
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Gmelin Handbook: Cl: MVol., 151, page 404 - 409
Gmelin Handbook: U: SVol.C8, 5.1.2, page 12 - 55
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Katz, J. J.; Rabinowitch, E.
The Chemistry of Uranium, Tl.1, McGraw-Hill, New York - Toronto - London 1951, S.355/82
in methanol
addn. of ligand soln. to a hot stirred soln. of ZnCl2; cooled slowly to room temp., crystn., filtered, washed (MeOH), dried at 70°C in vac. overnight, elem. anal.;
参考文献
Nanjappan, Palaniappan; Czarnik, Anthony W.
Journal of the American Chemical Society, 1987 , vol. 109, # 6 p. 1826 - 1833
in ethanol; benzene
byproducts: (C6H5)ZnCl; (N2); refluxing a mixt. of alcoholic soln. of ZnCl2 and benzene soln. of (C6H5)3Sb for 4 h; evapn. of solvent in vac. (to 3/4 of volume); filtration; e)); isolating of (C6H5)2SbCl from the ppt. (filtration, drying in vac); removal of solvent (reduced pressure); elem. anal.;
参考文献
Sharma, Hemant K.; Dubey, S. N.; Puri, D. M.
Journal of the Indian Chemical Society, 1983 , vol. 60, p. 696 - 698
