1: 1-bromo-2-methyl benzene With n-butyllithium in tetrahydrofuran
T=-78°C; 1 h; Sealed tubeInert atmosphere;
2: zinc(II) chloride in tetrahydrofuran
T=-78 - 20°C; Sealed tubeInert atmosphere;
参考文献
Dennis, Joseph M.; Calyore, Catherine M.; Sjoholm, Jessica S.; Lutz, J. Patrick; Gair, Joseph J.; Johnson, Jeffrey B.
Synlett, 2013 , vol. 24, # 19 art. no. ST-2013-S0592-L, p. 2567 - 2570
