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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
76465-53-7
合成路线
（共 9 条）
76465-53-7
→
反应条件
111077-41-9
反应条件
1: 88 percent / mercuric oxide, methanolic potassium hydroxide / diethyl ether 2: 60 percent / dimethylformamide / 50 °C View Scheme
参考文献
Iwamura, Michiko; Ishikawa, Touru; Koyama, Yukiyoshi; Sakuma, Keisuke; Iwamura, Hiizu
Tetrahedron Letters, 1987 , vol. 28, # 6 p. 679 - 682
76465-53-7
→
反应条件
24463-15-8
1-芘甲醇
反应条件
1: 88 percent / mercuric oxide, methanolic potassium hydroxide / diethyl ether 2: 60 percent / dimethylformamide / 50 °C 3: dioxane / 0.5 h / Irradiation View Scheme
参考文献
Iwamura, Michiko; Ishikawa, Touru; Koyama, Yukiyoshi; Sakuma, Keisuke; Iwamura, Hiizu
Tetrahedron Letters, 1987 , vol. 28, # 6 p. 679 - 682
76465-53-7
→
反应条件
155386-57-5
7-叔丁基-1-甲基芘
反应条件
1: KOH / bis-(2-hydroxy-ethyl) ether / 3 h / 180 °C 2: 80 percent / AlCl3 / CH2Cl2 / 2 h / Ambient temperature View Scheme
参考文献
Yamato, Takehiko; Fujimoto, Masakazu; Nagano, Yoshiaki; Miyazawa, Akira; Tashiro, Masashi
Organic Preparations and Procedures International, 1997 , vol. 29, # 3 p. 321 - 330
76465-53-7
→
反应条件
2381-21-7
1-甲基芘
反应条件
potassium hydroxide in diethylene glycol T=180°C; 3 h; Yield given;
参考文献
Yamato, Takehiko; Fujimoto, Masakazu; Nagano, Yoshiaki; Miyazawa, Akira; Tashiro, Masashi
Organic Preparations and Procedures International, 1997 , vol. 29, # 3 p. 321 - 330
76465-53-7
→
反应条件
78377-23-8
1-芘基二氮杂甲烷
反应条件
potassium hydroxide; mercury(II) oxide in diethyl ether
参考文献
Iwamura, Michiko; Ishikawa, Touru; Koyama, Yukiyoshi; Sakuma, Keisuke; Iwamura, Hiizu
Tetrahedron Letters, 1987 , vol. 28, # 6 p. 679 - 682
76465-53-7
→
反应条件
91385-15-8
反应条件
1: 88 percent / mercuric oxide, methanolic potassium hydroxide / diethyl ether 2: 60 percent / dimethylformamide / 50 °C 3: 95 percent / 0.5 h / Irradiation; recovery of carboxylic acids from their 1-pyrenylmethyl esters View Scheme
参考文献
Iwamura, Michiko; Ishikawa, Touru; Koyama, Yukiyoshi; Sakuma, Keisuke; Iwamura, Hiizu
Tetrahedron Letters, 1987 , vol. 28, # 6 p. 679 - 682
76465-53-7
→
反应条件
64401-21-4
1,3-二甲基芘
反应条件
1: KOH / bis-(2-hydroxy-ethyl) ether / 3 h / 180 °C 2: 80 percent / AlCl3 / CH2Cl2 / 2 h / Ambient temperature 3: 82 percent / TiCl4 / CH2Cl2 / 2 h / Ambient temperature 4: N2H4*H2O / toluene; bis-(2-hydroxy-ethyl) ether / 1 h / Heating 5: KOH / bis-(2-hydroxy-ethyl) ether / 3 h / 180 °C 6: 78 percent / Nafion-H, toluene / 12 h / Heating View Scheme
参考文献
Yamato, Takehiko; Fujimoto, Masakazu; Nagano, Yoshiaki; Miyazawa, Akira; Tashiro, Masashi
Organic Preparations and Procedures International, 1997 , vol. 29, # 3 p. 321 - 330
76465-53-7
→
反应条件
111077-44-2
反应条件
Multi-step reaction with 2 steps 1: 88 percent / mercuric oxide, methanolic potassium hydroxide / diethyl ether2: dimethylformamide
参考文献
Iwamura, Michiko; Ishikawa, Touru; Koyama, Yukiyoshi; Sakuma, Keisuke; Iwamura, Hiizu Tetrahedron Letters, 1987 , vol. 28, # 6 p. 679 - 682
76465-53-7
→
反应条件
111077-45-3
反应条件
Multi-step reaction with 2 steps 1: 88 percent / mercuric oxide, methanolic potassium hydroxide / diethyl ether2: dimethylformamide
参考文献
Iwamura, Michiko; Ishikawa, Touru; Koyama, Yukiyoshi; Sakuma, Keisuke; Iwamura, Hiizu Tetrahedron Letters, 1987 , vol. 28, # 6 p. 679 - 682
