sulfuric acid in water T=5°C;

1.1: tetrabutylammomium bromide; sodium hydroxide / water / 20 °C / Large scale reaction 1.2: 4 h / 0 - 3 °C 2.1: sodium hydride / ethylene glycol dimethyl ether; toluene; mineral oil 2.2: 4 h / 80 °C 3.1: hydrogenchloride; water / 4 h / 60 °C / pH 9 - 10 4.1: hydrogenchloride / dichloromethane; water / 8 h / 25 °C 5.1: sodium hydrogencarbonate / acetone / 60 °C 6.1: sodium tetrahydroborate; potassium hydroxide / ethanol; water / 13 h / 20 °C / Reflux 6.2: pH 5 - 6 View Scheme

diborane in tetrahydrofuran 10 h; Heating;

暂无反应条件数据

1: 87 percent / sulfuric acid / H2O / 5 °C 2: 70 percent / nitric acid; sulfuric acid / 3 h / 20 °C 3: 70 percent / thionylchloride / CCl4 / 4 h / 20 °C View Scheme

1: ethanolic sodium ethylate 2: HCl; acetic acid View Scheme

[RhCl(η2:η2-cycloocta-1,5-diene)]2 in 2-cyclohexylethanol T=160°C; 15 h; Inert atmosphere;

hydrogenchloride; potassium cyanide in tetrahydrofuran; methanol; water