反应条件
in neat (no solvent)
heating of mixt. of NaCl/NH4Cl (ratio NaCl:NH4Cl 1:1 plus Cu shot, stainless steel reactor, 110°C, 4 h, N2 flow), cooling (55 - 60°C), introduction of F2 in He (2 - 4 h); collection in cold trap (liq. N2 temp.), distn. (cold traps, -80, -118 and -196°C);
参考文献
Arunan, E.; Liu, C. P.; Setser, D. W.; Gilbert, J. V.; Coombe, R. D.
Journal of Physical Chemistry, 1994 , vol. 98, # 2 p. 494 - 501
