in neat (no solvent) byproducts: Cl2; react. starting at 120 °C, react. at higher temp. with detonation; formation of a grey-black compound with composition PN impured with Cl2;;
参考文献
Bulletin de la Societe Chimique de France, , vol. 53, p. 692 - 697
in dichloromethane; triethylamine; acetonitrile mixt. of the Fe complex in CH3CN and Na benzoate stirred for 0.5 h; mixt. of BICOH in CH3CN/CH2Cl2 and Et3N stirred for 1 h and added to first mixt.; reaction mixt. stirred for 1 h; filtration, solvents removed in vac.; solid washed with hexane/CHCl3; resulting oil dried overnight under vac.; recrystn. from CH3CN; elem. anal.;
参考文献
Gorun, Sergiu M.; Lippard, Stephen J.
Inorganic Chemistry, 1988 , vol. 27, p. 149 - 156
