反应条件
in tetrahydrofuran; hexane addn. of Na-compound (prepared from (C5H5)Fe(CO)3 and excess 3percent Na-amalgam) in THF to i-Pr3GeHgBr (prepared from (i-PrGe)2Hg and Br2) in hexane at -40°C; pptn. (NaBr), replacing of solvents in the mother-liquor by hexane, pptn. of Fe-compound, isolation of (i-Pr3Ge)2Hg by fractionation of the soln. in vac.;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 36, p. 1291 - 1292
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , vol. 36, p. 1397 - 1398