Beilstein; Schlun
Justus Liebigs Annalen der Chemie, 1865 , vol. 133, p. 249
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Loessner
Journal fuer Praktische Chemie (Leipzig), 1876 , vol. <2> 13, p. 427
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Gerhardt
Traite de chimie organique, Bd. III <Paris 1854> S. 214
in further solvent(s) byproducts: SbCl3; treatment of chlorophosphazene in CHCl2CHCl2 with SbF3, stepwise addn. of SbCl5 to refluxing soln. (stirring), refluxing for 40-80 min (GLC-control); decantation, evapn. (vac.), repeated extn. and evapn. (pentane, then pentane or CH2Cl2), gas chromy., recrystn. (pentane, -80°C); elem. anal.;
参考文献
Paddock, Norman L.; Patmore, David J.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1976 , p. 1029 - 1031
in neat (no solvent) byproducts: Cl2; Cl2O6 added to SbCl5 at -180°C in Pyrex reactor, mixt. allowed to warm slowly to 10°C, gases removed periodically; unreacted SbCl5 pumped out, elem. anal.;
参考文献
Belin, C.H.; Chaabouni, M.; Pascal, J.L.; Potier, J.
Inorganic Chemistry, 1982 , vol. 21, p. 3557 - 3560
Barral
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1898 , vol. 126, p. 908
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1904 , vol. 138, p. 909,980