in dichloromethane byproducts: SO2, N2; stirring mixt. of Te-compd. and SbCl5 (molar ratio 2.1:1.5) in abs. CH2Cl2 at -80°C in a sealed tube (12 h); filtration of pptn. in absence of air and moisture, washing (CH2Cl2), concn. of combined filtrates by removal of solvent in vac. to half of vol., crystn. after few weeks;
参考文献
Haas, A.; Pohl, R.
European Journal of Solid State and Inorganic Chemistry, 1992 , vol. 29, p. 791 - 798
in neat (no solvent) adding components separately into sealed tube and heating to 95 to 105°C;;
参考文献
Fireman, E.; Fireman, P.
American Chemical Journal, 1903 , vol. 30, p. 116 - 133
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Gmelin Handbook: P: MVol.C, 230, page 527 - 529
