under exclusion of moisture; I2 is dissolved in SbCl5 at 50-60°C, 1 d; the solvent is sucked off from the crystals, the crystals are washed (CCl4), elem. anal.;
参考文献
Pohl, Siegfried; Saak, Wolfgang
Zeitschrift fuer Naturforschung, Teil B: Anorganische Chemie, Organische Chemie, 1981 , vol. 36, # 3 p. 283 - 288
in tetrachloromethane under N2; SbCl5 reacted with Ph3SbS (molar ratio 1:1) in CCl4 at -20°C; detd. by IR and (1)H NMR spectra; mixt. of Ph3SbS and Ph3SbCl2 obtained;
参考文献
Corcoran, Sarah M.; Levason, William; Patel, Rina; Reid, Gillian
Inorganica Chimica Acta, 2005 , vol. 358, # 4 p. 1263 - 1268
Lacher et al.
Journal of the American Chemical Society, 1949 , vol. 71, p. 1333
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Lewis; Naylor
Journal of the American Chemical Society, 1947 , vol. 69, p. 1969
