in dichloromethane
by dropwise addn. of a slight excess of a 10percent soln. of SbCl5 in CH2Cl2 to a 10percent soln. of the org. compd. in the same solvent at 0°C under N2 or Ar;; the pptd. complex was washed with a little dry CCl4 and sealed in a glass ampoule;;
参考文献
Rupp-Bensadon, Joyce; Lucken, Edwin A. C.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1983 , p. 19 - 24