Cotton, J. D.; Waddington, T. C.
Journal of the Chemical Society [Section] A: Inorganic, Physical, Theoretical, 1966 , p. 793 - 797
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Gmelin Handbook: S: SVol.4a/b, 1.3.13.3, page 308 - 309
in neat (no solvent) (CH3)3SiNHTeF5 and PF5 stirred for 14 h at room temp.; products distilled under dynamic vac. through -30 (H2NTeF5), -78 (F3P=NTeF5) and -196°C ((CH3)3SiF and PF5) trap; elem. anal.;
参考文献
Hartl, Hans; Huppmann, Peter; Lentz, Dieter; Seppelt, Konrad
Inorganic Chemistry, 1983 , vol. 22, p. 2183 - 2187
in nitromethane addn. of PF5 to a soln. of anhyd. HF and HNO3 (or alkylnitrate) in nitromethane at -20 to 0°C;; filtn.; washing with CHCl3 and nitromethane and drying in vac.;;
in nitric acid PF5 concn. in excess of ca. 5 wtpercent; pptd. from soln.;
参考文献
Addison, C. Clifford; Bailey, John W.; Bruce, Simon H.; Dove, Michael F. A.; Hibbert, Richard C.; Logan, Norman
Polyhedron, 1983 , vol. 2, p. 651 - 656
