Morachalcone A合成路线 （共 7 条）
反应条件
hydrogenchloride in tetrahydrofuran; isopropyl alcohol T=25°C; 18 h;
参考文献
Brandt, Drew R.; Pannone, Kristina M.; Romano, Joseph J.; Casillas, Eduard G.
Tetrahedron, 2013 , vol. 69, # 47 p. 9994 - 10002
反应条件
1: 96 percent / diisopropylethylamine / CH2Cl2 / 3 h / 0 - 25 °C 2: 66 percent / KOH / ethanol / 18 h / 25 °C 3: 87 percent / potassium carbonate / acetone / 18 h / Heating 4: 23 percent / Florisil(R) / toluene / 8 h / 100 °C 5: 46 percent / aq. HCl / tetrahydrofuran; propan-2-ol / 18 h / 25 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 46, # 13 p. 2323 - 2326
反应条件
1: 66 percent / KOH / ethanol / 18 h / 25 °C 2: 87 percent / potassium carbonate / acetone / 18 h / Heating 3: 23 percent / Florisil(R) / toluene / 8 h / 100 °C 4: 46 percent / aq. HCl / tetrahydrofuran; propan-2-ol / 18 h / 25 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 46, # 13 p. 2323 - 2326
反应条件
1: 82 percent / sodium hydride / tetrahydrofuran / 18 h / 65 °C 2: 66 percent / KOH / ethanol / 18 h / 25 °C 3: 87 percent / potassium carbonate / acetone / 18 h / Heating 4: 23 percent / Florisil(R) / toluene / 8 h / 100 °C 5: 46 percent / aq. HCl / tetrahydrofuran; propan-2-ol / 18 h / 25 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 46, # 13 p. 2323 - 2326
反应条件
1: 66 percent / KOH / ethanol / 18 h / 25 °C 2: 87 percent / potassium carbonate / acetone / 18 h / Heating 3: 23 percent / Florisil(R) / toluene / 8 h / 100 °C 4: 46 percent / aq. HCl / tetrahydrofuran; propan-2-ol / 18 h / 25 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 46, # 13 p. 2323 - 2326
反应条件
1: 87 percent / potassium carbonate / acetone / 18 h / Heating 2: 23 percent / Florisil(R) / toluene / 8 h / 100 °C 3: 46 percent / aq. HCl / tetrahydrofuran; propan-2-ol / 18 h / 25 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 46, # 13 p. 2323 - 2326
反应条件
1: 23 percent / Florisil(R) / toluene / 8 h / 100 °C 2: 46 percent / aq. HCl / tetrahydrofuran; propan-2-ol / 18 h / 25 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 46, # 13 p. 2323 - 2326
