cesium hydroxide; 4 Angstroem MS in N,N-dimethyl-formamide
T=23°C; 62 h;
参考文献
Honaker, Matthew T.; Sandefur, Benjamin J.; Hargett, James L.; McDaniel, Alicia L.; Salvatore, Ralph Nicholas
Tetrahedron Letters, 2003 , vol. 44, # 46 p. 8373 - 7377
1: sec.-butyllithium; S-(-)-[1-(3-methoxyphenyl)ethyl]-N,N-dimethylamine T=-50°C; 4 h;
2: chloro-diphenylphosphine T=-50 - 20°C; Further stages. Title compound not separated from byproducts.;
参考文献
Alberico, Elisabetta; Braun, Wolfgang; Calmuschi-Cula, Beatrice; Englert, Ulli; Salzer, Albrecht; Totev, Daniel
European Journal of Inorganic Chemistry, 2007 , # 31 p. 4923 - 4945