1-辛烷硫代磺酸 S-辛基酯合成路线 （共 9 条）
反应条件
iodine; triphenylphosphine in benzene 0.25 h; Ambient temperature; Yield given;
参考文献
Oae, Shigeru; Togo, Hideo
Synthesis, 1981 , # 5 p. 371 - 373
反应条件
zinc dichromate trihydrate in acetonitrile
T=20°C; 0.166667 h; chemoselective reaction;
参考文献
Sobhani, Sara; Aryanejad, Sima; Maleki, Mahdi Faal
Synlett, 2011 , # 3 art. no. D28310ST, p. 319 - 322
反应条件
zinc in tetrachloromethane
T=22 - 24°C; 48 h;
参考文献
Freeman, Fillmore; Angeletakis, Christos N.; Keindl, Monica C.
Journal of Organic Chemistry, 1984 , vol. 49, # 3 p. 454 - 458
反应条件
hydrogenchloride; water; chlorine
T=6 - 20°C; 6 - 9 h; Industry scale;
参考文献
Ollivier, Jean; Haurat, Gisele
Patent: US2004/15019 A1, 2004 ;
Location in patent: Page 2-3 ;
反应条件
water; chlorine
Industry scale;
参考文献
Ollivier, Jean; Haurat, Gisele
Patent: US2004/15019 A1, 2004 ;
Location in patent: Page 3 ;
反应条件
dihydrogen peroxide in acetic acid
Ambient temperature;
参考文献
Oae, Shigeru; Togo, Hideo
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 12 p. 3802 - 3812
反应条件
in water; acetone
Heating;
参考文献
Weidner,J.P.; Block,S.S.
J. Med. Chem., 1964 , vol. 7, p. 671 - 673
参考文献
Freeman, Fillmore; Keindl, Monica C.
Synthesis, 1984 , # 6 p. 500 - 502
反应条件
sodium hydroxide; tetra-(n-butyl)ammonium iodide; trifluoroacetic anhydride
1.) CH2Cl2, 68h, room temp., 2.) room temp.; Yield given. Multistep reaction;
参考文献
Numata Tatsuo,; Awano Hiroshi,; Oae Shigeru
Tetrahedron Letters, 1980 , vol. 21, p. 1235 - 1238
