N-乙酰基-L-半胱氨酸甲酯合成路线 （共 23 条）
反应条件
sodium hydrogencarbonate in methanol; water T=20°C; 16 h; Inert atmosphere;
参考文献
Kuramochi, Kouji; Sunoki, Takashi; Tsubaki, Kazunori; Mizushina, Yoshiyuki; Sakaguchi, Kengo; Sugawara, Fumio; Ikekita, Masahiko; Kobayashi, Susumu
Bioorganic and Medicinal Chemistry, 2011 , vol. 19, # 14 p. 4162 - 4172
反应条件
T=20°C; pH=7; 24 h; aq. phosphate bufferInert atmosphere;
参考文献
Kuramochi, Kouji; Sunoki, Takashi; Tsubaki, Kazunori; Mizushina, Yoshiyuki; Sakaguchi, Kengo; Sugawara, Fumio; Ikekita, Masahiko; Kobayashi, Susumu
Bioorganic and Medicinal Chemistry, 2011 , vol. 19, # 14 p. 4162 - 4172
反应条件
sodium hydrogencarbonate in methanol; water T=20°C; 0.333333 h;
参考文献
Kuramochi, Kouji; Yukizawa, Shunsuke; Ikeda, Seiki; Sunoki, Takashi; Arai, Satoshi; Matsui, Rie; Morita, Akinori; Mizushina, Yoshiyuki; Sakaguchi, Kengo; Sugawara, Fumio; Ikekita, Masahiko; Kobayashi, Susumu
Bioorganic and Medicinal Chemistry, 2008 , vol. 16, # 9 p. 5039 - 5049
反应条件
sodium hydrogencarbonate in methanol; water T=20°C; 24 h;
参考文献
Kuramochi, Kouji; Yukizawa, Shunsuke; Ikeda, Seiki; Sunoki, Takashi; Arai, Satoshi; Matsui, Rie; Morita, Akinori; Mizushina, Yoshiyuki; Sakaguchi, Kengo; Sugawara, Fumio; Ikekita, Masahiko; Kobayashi, Susumu
Bioorganic and Medicinal Chemistry, 2008 , vol. 16, # 9 p. 5039 - 5049
反应条件
1,2-diphenyl-1-keto-2,2-dimethoxyethane in dimethyl sulfoxide T=20 - 40°C; 2 h; UV-irradiation;
参考文献
Minozzi, Matteo; Monesi, Alessandro; Nanni, Daniele; Spagnolo, Piero; Marchetti, Nicola; Massi, Alessandro
Journal of Organic Chemistry, 2011 , vol. 76, # 2 p. 450 - 459
反应条件
1,2-diphenyl-1-keto-2,2-dimethoxyethane in dimethyl sulfoxide T=20 - 40°C; 2 h; UV-irradiation; optical yield given as percent de;
参考文献
Minozzi, Matteo; Monesi, Alessandro; Nanni, Daniele; Spagnolo, Piero; Marchetti, Nicola; Massi, Alessandro
Journal of Organic Chemistry, 2011 , vol. 76, # 2 p. 450 - 459
反应条件
sodium hydrogencarbonate in water; acetonitrile 3.5 h;
参考文献
Black, R. M.; Brewster, K.; Clarke, R. J.; Harrison, J. M.
Phosphorus, Sulfur and Silicon and the Related Elements, 1992 , vol. 71, # 1-4 p. 49 - 58
反应条件
sodium hydrogencarbonate in acetonitrile 4 h;
参考文献
Black, R. M.; Brewster, K.; Clarke, R. J.; Harrison, J. M.
Phosphorus, Sulfur and Silicon and the Related Elements, 1992 , vol. 71, # 1-4 p. 49 - 58
反应条件
zinc diacetate; trifluoroacetic acid in water; N,N-dimethyl-formamide; acetonitrile 24 h;
参考文献
Kale; Raab; Yu; Dean; Distefano
Journal of the American Chemical Society, 2001 , vol. 123, # 19 p. 4373 - 4381
反应条件
1: (2R)-2-acetylamino-2-methoxycarbonylethanethiol With sodium hydride in methanol; mineral oil Cooling with iceInert atmosphere; 2: 1-vinylbenzene 3,4-oxide in methanol; mineral oil; pentane 2 h; Inert atmosphere;
参考文献
Linhart, Igor; Mraz, Jaroslav; Scharff, Jan; Krouzelka, Jan; Duskova, Sarka; Nohova, Hana; Vodickova, L'udmila
Chemical Research in Toxicology, 2010 , vol. 23, # 1 p. 251 - 257
