2,2'-联-4-勒皮啶合成路线 （共 13 条）
反应条件
2,6-dimethylpyridine; sodium perchlorate in 1,2,3,4-tetrahydro-naphthalene; acetonitrile electrolyse (2,2,6,6-tetramethylpiperidinyl-1-oxyl (TEMPO)-modified graphite felt electrode);
参考文献
Kashiwagi, Yoshitomo; Ono, Hiroaki; Osa, Tetsuo
Chemistry Letters, 1993 , # 2 p. 257 - 260
反应条件
triethylamine; palladium diacetate T=100°C; 24 h;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 30, # 10 p. 3647 - 3656
反应条件
1: 93 percent / NaI, 56 percent HI / butan-2-one / 24 h / Heating 2: 6 percent / Et3N / Pd(OAc)2 / 24 h / 100 °C View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 30, # 10 p. 3647 - 3656
反应条件
trichlorophosphate 24 h; Heating;
参考文献
Molina; Alajarin; Sanchez-Andrada
Synthesis, 1993 , # 2 p. 225 - 228
反应条件
methylmagnesium bromide in tetrahydrofuran 0.25 h; Ambient temperature;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 62, # 12 p. 3848 - 3850
反应条件
methylmagnesium bromide in tetrahydrofuran 0.25 h; Ambient temperature;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 62, # 12 p. 3848 - 3850
反应条件
triethylamine; palladium diacetate T=100°C; 24 h;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 30, # 10 p. 3647 - 3656
反应条件
in diethylene glycol dimethyl ether 2 h; Heating;
参考文献
Kobayashi, Kazuhiro; Yonemori, Junpei; Matsunaga, Akihiro; Kitamura, Taichi; Miyuki, Tanmatsu; Morikawa, Osamu; Konishi, Hisatoshi
Heterocycles, 2001 , vol. 55, # 1 p. 33 - 36
反应条件
1: toluene / Heating 2: Et3N; POCl3 / tetrahydrofuran 3: 75 percent / bis-(2-methoxy-ethyl) ether / 2 h / Heating View Scheme
参考文献
Heterocycles, , vol. 55, # 1 p. 33 - 36
反应条件
triethylamine; palladium diacetate T=100°C; 24 h;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 30, # 10 p. 3647 - 3656
