2-(4-甲氧基苯基)-N,N-二甲基硫代乙酰胺合成路线 （共 10 条）
反应条件
1: aqueous-alcoholic hydrochloric acid / 20 °C / elektrolytische Reduktion an Bleikathode 2: hydrobromic acid; red phosphorus / 110 °C View Scheme
参考文献
Kindler
Archiv der Pharmazie (Weinheim, Germany), 1927 , p. 390,400
Chem. Zentralbl., 1924 , vol. 95, # II p. 1404
参考文献
Kindler
Patent: DE405675 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 14, p. 372
Full Text Show Details
Kindler
Justus Liebigs Annalen der Chemie, 1923 , vol. 431, p. 213
Chem. Zentralbl., 1923 , vol. 94, # II p. 403
参考文献
Kindler
Patent: DE405675 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 14, p. 372
Full Text Show Details
Kindler
Justus Liebigs Annalen der Chemie, 1923 , vol. 431, p. 213
Chem. Zentralbl., 1923 , vol. 94, # II p. 403
反应条件
sulfur; copper acetylacetonate; pentanal; potassium carbonate
T=110°C; 24 h; Schlenk technique;
参考文献
Qu, Yanyang; Li, Zhengkai; Xiang, Haifeng; Zhou, Xiangge
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 16 p. 3141 - 3146
反应条件
in methanol
5 h; Ambient temperature;
参考文献
Ogura, Katsuyuki; Ito, Yoko; Tsuchihashi, Gen-ichi
Synthesis, 1980 , # 9 p. 736 - 739
参考文献
Schroth, Werner; Andersch, Joerg
Synthesis, 1989 , # 3 p. 202 - 204
反应条件
sulfur
T=170 - 180°C; im Rohr;
参考文献
Kindler
Patent: DE405675 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 14, p. 372
Full Text Show Details
Kindler
Justus Liebigs Annalen der Chemie, 1923 , vol. 431, p. 213
Chem. Zentralbl., 1923 , vol. 94, # II p. 403
反应条件
1: 80 percent / 110 °C
2: 90 percent / methanol / 5 h / Ambient temperature
View Scheme
参考文献
Ogura, Katsuyuki; Ito, Yoko; Tsuchihashi, Gen-ichi
Synthesis, 1980 , # 9 p. 736 - 739
参考文献
Androsov; Petrov; Shchipalkin
Russian Journal of Organic Chemistry, 2007 , vol. 43, # 12 p. 1870 - 1873
反应条件
hydrogenchloride
T=20°C; elektrolytische Reduktion an Bleikathode;
参考文献
Kindler
Archiv der Pharmazie (Weinheim, Germany), 1927 , p. 390,400
Chem. Zentralbl., 1924 , vol. 95, # II p. 1404
