2-(溴甲基)吗啉-4-羧酸叔丁酯合成路线 (共 2 条)
反应条件
carbon tetrabromide; triphenylphosphine in dichloromethane
T=-20 - 20°C; 19.5 h;
参考文献
SMITHKLINE BEECHAM CORPORATION
Patent: WO2007/58850 A2, 2007 ;
Location in patent: Page/Page column 44 ;
WO 2007/058850 A2
反应条件
triphenylphosphine in dichloromethane
参考文献
Munson, Mark; Mareska, David A.; Kim, Youngboo; Groneberg, Robert D.; Rizzi, James; Rodriguez, Martha; Kim, Ganghyeok; Vigers, Guy; Rao, Chang; Balachari, Devan; Harvey, Darren
Patent: US2004/192653 A1, 2004 ;
US 20040192653 A1