反应条件
1: 1.) CuCN / 1.) THF, -23 deg C, 5 h, 2.) THF, from -23 deg C to RT, 1 h 2: 40 percent / NaOMe / methanol / 96 h / Ambient temperature 3: 95 percent / m-chloroperbenzoic acid, disodium hydrogenphosphate / CH2Cl2 / 24 h / Ambient temperature 4: 98 percent / LiAlH4 / diethyl ether / 2 h / Ambient temperature 5: 100 percent / KH / tetrahydrofuran / 0.5 h / Ambient temperature View Scheme
参考文献
Journal of Organometallic Chemistry, , vol. 271, # 1-3 p. 281 - 288
