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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
4-氟苯乙炔
合成路线
（共 110 条）
766-98-3
4-氟苯乙炔
+
348-52-7
2-氟碘苯
→
反应条件
反应条件
triethylamine; palladium complex immobilised on silica gel in various solvent(s) T=70°C; Sonogashira coupling; 12 h;
参考文献
Bandini, Marco; Luque, Rafael; Budarin, Vitaly; Macquarrie, Duncan J.
Tetrahedron, 2005 , vol. 61, # 41 p. 9860 - 9868
766-98-3
4-氟苯乙炔
+
107047-10-9
→
反应条件
反应条件
4-(N,N-dimethlyamino)pyridine; copper(l) iodide in acetonitrile T=20°C; 72 h; Darkness;
参考文献
Smith, Nicholas W.; Polenz, Bradley P.; Johnson, Shawna B.; Dzyuba, Sergei V.
Tetrahedron Letters, 2010 , vol. 51, # 3 p. 550 - 553
766-98-3
4-氟苯乙炔
+
768-60-5
4-乙炔基苯甲醚
→
反应条件
反应条件
piperidine; C34H22Cl4CoCu2N10O4(1-)*C8H20N(1+); oxygen in neat (no solvent) T=25°C; 4 h;
参考文献
Srivastava, Sumit; Ali, Afsar; Tyagi, Adish; Gupta, Rajeev
European Journal of Inorganic Chemistry, 2014 , # 12 p. 2113 - 2123
766-98-3
4-氟苯乙炔
+
77152-08-0
→
反应条件
反应条件
N,N,N',N,-tetramethylethylenediamine; phosphoric acid in N,N-dimethyl-formamide T=20°C; 1 h; TimeSolventReagent/catalyst;
参考文献
Serizawa, Hiroki; Aikawa, Kohsuke; Mikami, Koichi
Chemistry - A European Journal, 2013 , vol. 19, # 52 p. 17692 - 17697
766-98-3
4-氟苯乙炔
+
536-74-3
苯乙炔
→
反应条件
886-66-8
1,4-二苯基丁二炔
反应条件
piperidine; C34H22Cl4Cu2FeN10O4(1-)*C8H20N(1+); oxygen in neat (no solvent) T=25°C; 4 h; Catalytic behavior; Reagent/catalyst;
参考文献
Srivastava, Sumit; Ali, Afsar; Tyagi, Adish; Gupta, Rajeev
European Journal of Inorganic Chemistry, 2014 , # 12 p. 2113 - 2123
766-98-3
4-氟苯乙炔
→
反应条件
557083-83-7
反应条件
Y[bis(trimethylsilyl)amide]3; 4-chloro-aniline in toluene T=100°C; 17 h;
参考文献
Komeyama, Kimihiro; Kawabata, Tomonori; Takehira, Katsuomi; Takaki, Ken
Journal of Organic Chemistry, 2005 , vol. 70, # 18 p. 7260 - 7266
766-98-3
4-氟苯乙炔
→
反应条件
反应条件
anhydrous iron chloride; potassium tert-butylate; N,N-dimethylethylenediamine in toluene T=145°C; 2 h; Inert atmosphere; optical yield given as percent deregioselective reaction;
参考文献
Midya, Ganesh Chandra; Parasar, Bibudha; Dhara, Kalyan; Dash, Jyotirmayee
Organic and Biomolecular Chemistry, 2014 , vol. 12, # 11 p. 1812 - 1822
766-98-3
4-氟苯乙炔
+
122-78-1
苯乙醛
→
反应条件
572-52-1
反应条件
boron trifluoride diethyl etherate in 1,2-dichloro-ethane T=80°C; 15 h; Schlenk technique;
参考文献
Xiang, Shikai; Hu, Hao; Ma, Jing; Li, Yuanzhuo; Wang, Biqin; Feng, Chun; Zhao, Keqing; Hu, Ping; Chen, Xiaozhen
Science China Chemistry, 2013 , vol. 56, # 7 p. 945 - 951
766-98-3
4-氟苯乙炔
+
201230-82-2
→
反应条件
58755-90-1
反应条件
copper dichloride; palladium dichloride in 1,4-dioxane; water T=20°C; P=760 Torr; 4 h;
参考文献
Li, Jinheng; Li, Guoping; Jiang, Huanfeng; Chen, Mingcai
Tetrahedron Letters, 2001 , vol. 42, # 39 p. 6923 - 6924
766-98-3
4-氟苯乙炔
+
318-13-8
→
反应条件
60253-25-0
反应条件
2,4,5,7-tetrabromofluorescein in acetonitrile T=20°C; 12 h; Inert atmosphereIrradiation;
参考文献
Xiao, Tiebo; Dong, Xichang; Tang, Yanchi; Zhou, Lei
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 17 p. 3195 - 3199
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