in further solvent(s)
Electrochem. Process; electrofluorination in anhyd. HF for 6 h 40 min 15°C, helium flow rate 60 mL/min, U=5.8-8.0 V, i=2.9 A/dm2;
Silvey; Cady
Journal of the American Chemical Society, 1952 , vol. 74, p. 5792
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Clifford et al.
Journal of the Chemical Society, 1953 , p. 2372,2374
Russell, J. L.; Jache, A. W.
Journal of Fluorine Chemistry, 1976 , vol. 7, p. 205 - 220
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Gmelin Handbook: Se: SVol.A3, 17.3.2, page 292 - 293
in hydrogen fluoride
byproducts: CO2, N2, C; Electrolysis; 1 M soln. of semicarbazide in anhydrous liquid HF; 5.6-5.7 V; ratio of NF3 : CF4 depends on potential used;