in gaseous matrix Irradiation (UV/VIS); metal rod ablation with third harmonic of Nd:YAG laser, ablation plume entraining in supersonic expansion of 5percent NH3/Ar mixt., free-jet expansionskimming to well collimated molecular beam;
参考文献
Ma, Tongmei; Leung; Cheung
Journal of Physical Chemistry A, 2004 , vol. 108, # 25 p. 5333 - 5337
in neat (no solvent) expanding excess of NH3 into PClF2, standing for 3 min; removal of volatiles, fractional low-temp. distn. (vac., trap at 227 K);mass spectroscopy;
参考文献
Arnold, David E. J.; Rankin, David W. H.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1976 , p. 1130 - 1134
in chloroform; monofluoro-trichloromethane; benzene warming; product mixt. not sepd., detd. by NMR spectroscopy;
参考文献
Arnold, David E. J.; Cromie, Ernest R.; Rankin, David W. H.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1977 , p. 1999 - 2004
Calingaert; Soroos
Journal of Organic Chemistry, 1937 , vol. 2, p. 537 Anm.
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Gilman; Bailie
Journal of the American Chemical Society, 1939 , vol. 61, p. 731,734
