1-(3'-甲氧基联苯-4-基)乙酮合成路线 （共 15 条）
反应条件
sodium carbonate; palladium on activated charcoal in ethanol T=20°C; Suzuki-Miyaura cross-coupling; 3 h;
参考文献
Synthesis, , # 4 art. no. F15104SS, p. 537 - 542
反应条件
1-ethyl-2-pyrrolidinone; 4-(N,N-dimethlyamino)pyridine; phosphonic acid diethyl ester; nickel dichloride; zinc dibromide in tetrahydrofuran T=20°C; 2.5 h;
参考文献
Organic Letters, , vol. 7, # 22 p. 4871 - 4874
反应条件
sodium hydroxide; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran; water T=60°C; Suzuki-Miyaura cross-coupling; 24 h; Product distribution / selectivity;
参考文献
US2009/30238 A1, ;
Page/Page column 22-23 ;
反应条件
potassium carbonate; polymer-supported Pd catalyst FC 1032 in ethanol T=120°C; Suzuki coupling; 0.416667 h; microwave irradiation;
参考文献
Organic Letters, , vol. 6, # 16 p. 2793 - 2796
反应条件
potassium phosphate; triphenylphosphine; palladium diacetate in N,N-dimethyl-formamide T=90°C; 1 h;
参考文献
Tetrahedron Letters, , vol. 48, # 38 p. 6644 - 6647
反应条件
oxygen; palladium diacetate; potassium carbonate in PEG-400 T=20°C; Suzuki coupling; 6 h;
参考文献
Advanced Synthesis and Catalysis, , vol. 350, # 3 p. 501 - 508
反应条件
potassium fluoride; palladium diacetate; tris-(o-tolyl)phosphine in N,N-dimethyl-formamide T=120°C;
参考文献
Tetrahedron, , vol. 50, # 28 p. 8301 - 8316
反应条件
potassium phosphate; triphenylphosphine; palladium diacetate in N,N-dimethyl-formamide T=90°C; 1 h;
参考文献
Tetrahedron Letters, , vol. 48, # 15 p. 2707 - 2711
反应条件
morpholine; C31H45Cl2N3OPd; caesium carbonate in water T=110°C; Suzuki-Miyaura Coupling; 12 h; Inert atmosphere;
参考文献
Organic and Biomolecular Chemistry, , vol. 11, # 45 p. 7899 - 7906
反应条件
1: 3-methoxybromobenzene With magnesium in tetrahydrofuran 2: With zinc dibromide in tetrahydrofuran 3: para-bromoacetophenone With 4-(N,N-dimethlyamino)pyridine; phosphonic acid diethyl ester; nickel dichloride in tetrahydrofuran T=25°C; Negishi cross-coupling; 2.5 h;
参考文献
Tetrahedron, , vol. 62, # 32 p. 7521 - 7533
