3-(四氢呋喃-3-基)丙酸乙酯合成路线 (共 4 条)
反应条件
hydrogen; palladium 10 on activated carbon in ethanol 6 h;
参考文献
US2008/4302 A1, ;
Page/Page column 111 ;
US 20080004302 A1
反应条件
10 palladium on activated charcoal; hydrogen in ethyl acetate 2 h;
参考文献
Tetrahedron, , vol. 67, # 35 p. 6673 - 6678
反应条件
1: sodium hydroxide / dichloromethane; water / 16 h / 0 - 20 °C / Inert atmosphere 2: 10 palladium on activated charcoal; hydrogen / ethyl acetate / 2 h View Scheme
参考文献
Tetrahedron, , vol. 67, # 35 p. 6673 - 6678
反应条件
1.1: diisobutylaluminium hydride / hexane; dichloromethane / 6 h / 0 °C / Inert atmosphere 1.2: Inert atmosphere 2.1: pyridinium chlorochromate / dichloromethane / 3 h / 20 °C / Inert atmosphere View Scheme
参考文献
Kotoku, Naoyuki; Fujioka, Shinichi; Nakata, Chiaki; Yamada, Masaki; Sumii, Yuji; Kawachi, Takashi; Arai, Masayoshi; Kobayashi, Motomasa
Tetrahedron, 2011 , vol. 67, # 35 p. 6673 - 6678