1: 4-hydroxy-benzonitrile With sodium hydride in N,N-dimethyl-formamide T=0 - 20°C; 1 h; Inert atmosphere; 2: n-decyl iodide in N,N-dimethyl-formamide T=20°C; 3 h; Inert atmosphere;
参考文献
Nakamura, Kyosuke; Furumi, Seiichi; Takeuchi, Masayuki; Shibuya, Tetsuro; Tanaka, Ken
Journal of the American Chemical Society, 2014 , vol. 136, # 15 p. 5555 - 5558
tetrafluoroboric acid diethyl ether complex; N-bromosuccinmide in acetonitrile 24 h; Ambient temperatureother acids; bromination of phenols and anisoles with NBS in the presence or absence of strong acids; Product distribution;
参考文献
Berg; Newbery
Journal of the Chemical Society, 1949 , p. 642,645