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乙二醇
甲醛
63148-62-9
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二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
4-羟基苯甲腈
合成路线
（共 577 条）
767-00-0
4-羟基苯甲腈
→
反应条件
147821-49-6
O-乙基[[4-(3,4,5-三羟基-6-甲基四氢吡喃-2-基)氧基苯基]甲基氨基]硫代甲酸酯
反应条件
1: NaH / dimethylformamide / 16 h / Ambient temperature 2: LiAlH4 / diethyl ether / 24 h / Heating 3: Na2CO3 / acetone; H2O / 2.5 h / Ambient temperature 4: 91 percent / HCOOH, PPh3, Pd(OAc)2 / tetrahydrofuran / 4.5 h / Heating 5: 80 percent / NIS, MS, TfOH / CH2Cl2 / 2 h / -40 °C 6: H2 / Pd / methanol / 6 h / Ambient temperature 7: dimethylformamide / 2.5 h / 80 °C 8: 95 percent / NaOMe, MeOH / 0.75 h / Ambient temperature View Scheme
参考文献
Leuck, Michael; Kunz, Horst
Carbohydrate Research, 1998 , vol. 312, # 1-2 p. 33 - 44
767-00-0
4-羟基苯甲腈
→
反应条件
135420-42-7
反应条件
1: 100 percent / Na / ethanol / 24 h / Heating 2: 95 percent / HCl / CHCl3 / 192 h 3: 100 percent / NH4Cl / ethanol / 4 h / Heating 4: 86 percent / ethanol / Heating View Scheme
参考文献
Reynaud, Pierre; Brion, Jean-Daniel; Nguyen-Tri-Xuong, Emmanuel; Davrinche, Catherine; Pieri, Francois; Arnold-Guerin, Marie-Luce
European Journal of Medicinal Chemistry, 1989 , vol. 24, p. 427 - 434
767-00-0
4-羟基苯甲腈
→
反应条件
125880-54-8
反应条件
1: ethanol. NaOEt / 48 h / Heating 2: 84 percent / HNO3, trifluoroacetic acid / acetic anhydride / 24 h / 45 °C View Scheme
参考文献
Tidwell; Jones; Geratz; Ohemeng; Cory; Hall
Journal of Medicinal Chemistry, 1990 , vol. 33, # 4 p. 1252 - 1257
65512-08-5
+
767-00-0
4-羟基苯甲腈
→
反应条件
138631-41-1
反应条件
sodium hydride 1.) DMF, 1 h, 2.) DMF, RT, overnight; Yield given. Multistep reaction;
参考文献
Harper, Richard W.; Herron, David K.; Bollinger, Nancy G.; Sawyer, J. Scott; Baldwin, Ronald F.; et al.
Journal of Medicinal Chemistry, 1992 , vol. 35, # 7 p. 1191 - 1200
767-00-0
4-羟基苯甲腈
→
反应条件
161975-22-0
4-苄基硫代苯胺
反应条件
1: potassium carbonate / acetone / |Reflux 2: NaSH; magnesium chloride / N,N-dimethyl-formamide / 20 °C View Scheme
参考文献
Lee, Yun Suk; Kim, Hee; Kim, Young-Ho; Roh, Eun Joo; Han, Hogyu; Shin, Kye Jung
Bioorganic and Medicinal Chemistry Letters, 2012 , vol. 22, # 24 p. 7555 - 7561
767-00-0
4-羟基苯甲腈
→
反应条件
125880-76-4
4-[4-(4-甲脒基-2-硝基-苯氧基)丁氧基]-3-硝基-苯甲脒
反应条件
1: ethanol. NaOEt / 48 h / Heating 2: HNO3, trifluoroacetic acid / acetic anhydride / 24 h / 45 °C 3: HCl (gas) / CHCl3 / 24 h / Ambient temperature 4: ethanol. NH3 / 40 - 60 °C View Scheme
参考文献
Tidwell; Jones; Geratz; Ohemeng; Cory; Hall
Journal of Medicinal Chemistry, 1990 , vol. 33, # 4 p. 1252 - 1257
767-00-0
4-羟基苯甲腈
→
反应条件
135420-41-6
反应条件
1: 95 percent / Na / ethanol / 24 h / Heating 2: 90 percent / HCl / CHCl3 3: NH4Cl / ethanol / Heating 4: 87 percent / ethanol / Heating View Scheme
参考文献
Reynaud, Pierre; Brion, Jean-Daniel; Nguyen-Tri-Xuong, Emmanuel; Davrinche, Catherine; Pieri, Francois; Arnold-Guerin, Marie-Luce
European Journal of Medicinal Chemistry, 1989 , vol. 24, p. 427 - 434
767-00-0
4-羟基苯甲腈
→
反应条件
135420-40-5
反应条件
1: 95 percent / Na / ethanol / 24 h / Heating 2: 95 percent / HCl / CHCl3 3: NH4Cl / ethanol / Heating 4: 85 percent / ethanol / Heating View Scheme
参考文献
Reynaud, Pierre; Brion, Jean-Daniel; Nguyen-Tri-Xuong, Emmanuel; Davrinche, Catherine; Pieri, Francois; Arnold-Guerin, Marie-Luce
European Journal of Medicinal Chemistry, 1989 , vol. 24, p. 427 - 434
767-00-0
4-羟基苯甲腈
+
874-90-8
4-甲氧基苯甲腈
+
77-78-1
硫酸二甲酯
→
反应条件
17061-61-9
4-甲氧基苄胺盐酸盐
反应条件
nickel monoaluminide in N-sodium hydroxide; ethanol
参考文献
Burroughs Wellcome Co.
Patent: US3949089 A1, 1976 ;
767-00-0
4-羟基苯甲腈
→
反应条件
125575-13-5
反应条件
1: 95 percent / Na / ethanol / 24 h / Heating 2: 95 percent / HCl / CHCl3 3: NH4Cl / ethanol / Heating 4: 90 percent / ethanol / Heating View Scheme
参考文献
Reynaud, Pierre; Brion, Jean-Daniel; Nguyen-Tri-Xuong, Emmanuel; Davrinche, Catherine; Pieri, Francois; Arnold-Guerin, Marie-Luce
European Journal of Medicinal Chemistry, 1989 , vol. 24, p. 427 - 434
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