反-3,3,5-三甲基环己醇合成路线 （共 8 条）
反应条件
tert.-butylhydroperoxide; 3 A molecular sieve; 3,3,5c-trimethyl-cyclohexan-r-ol; zirconium tetra-n-propoxide in dichloromethane T=20°C; 7 h;
参考文献
Krohn, Karsten; Vinke, Ingeborg; Adam, Horst
Journal of Organic Chemistry, 1996 , vol. 61, # 4 p. 1467 - 1472
反应条件
2,5-dimethyl-2,5-dihydroxy hexane; nickel diacetate; sodium hydride; magnesium bromide in tetrahydrofuran T=63°C; 3 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Feghouli, G.; Vanderesse, R.; Fort, Y.; Caubere, P.
Tetrahedron Letters, 1988 , vol. 29, # 12 p. 1383 - 1384
参考文献
Alkonyi
Chemische Berichte, 1960 , vol. 93, p. 758,759
反应条件
2,5-dimethyl-2,5-dihydroxy hexane; nickel diacetate; sodium hydride; magnesium bromide in tetrahydrofuran
T=63°C; 3 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Feghouli, G.; Vanderesse, R.; Fort, Y.; Caubere, P.
Tetrahedron Letters, 1988 , vol. 29, # 12 p. 1383 - 1384
反应条件
lithium aluminium tetrahydride; [6-(N-Decylamino)-4-hydroxymethylindole]; 2,4,6-tri-(tert-butyl)phenol in diethyl ether
0.5 h; Ambient temperaturevariation of time, temperature, also with 4-tert-butylcyclohexanone; Product distributionMechanism;
参考文献
Alkonyi
Chemische Berichte, 1959 , vol. 92, p. 1130,1134
反应条件
Gleichgewichtsgemisch;
参考文献
Hardy; Wicker
Journal of the American Chemical Society, 1958 , vol. 80, p. 640
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Eliel; Haubenstock
Journal of Organic Chemistry, 1961 , vol. 26, p. 3504
参考文献
Alkonyi
Chemische Berichte, 1960 , vol. 93, p. 758,759
参考文献
Alkonyi
Chemische Berichte, 1960 , vol. 93, p. 758,759
