1: 63 percent / hydroxylamine hydrochloride, KOH / ethanol; methanol / 1 h / 40 °C 2: 94 percent / 98percent hydrazine hydrate / 5percent Pd/C / ethanol / 2 h / 50 °C 3: 56 percent / ethanol; H2O / 1 h 4: 63 percent / performic acid 5: 57 percent / POCl3 View Scheme

1: 94 percent / 98percent hydrazine hydrate / 5percent Pd/C / ethanol / 2 h / 50 °C 2: 56 percent / ethanol; H2O / 1 h 3: 63 percent / performic acid 4: 57 percent / POCl3 View Scheme

trichlorophosphate

1: 56 percent / ethanol; H2O / 1 h 2: 63 percent / performic acid 3: 57 percent / POCl3 View Scheme

trichlorophosphate

phosphorus pentachloride; trichlorophosphate Yield given. Multistep reaction;